MassBank Record: MSBNK-RIKEN_NPDepo-NGA03818
ACCESSION: MSBNK-RIKEN_NPDepo-NGA03818
RECORD_TITLE: Guan-fu base Y; LC-ESI-QQQ; MS2; Frag=135.0V CID@10.0; [M+HCOO]-
DATE: 2018.04.04
AUTHORS: Nogawa T, Okano A, CSRS, RIKEN
LICENSE: CC BY
COMMENT: Origin: Plant
COMMENT: Formula(Parent): C22H29NO5
COMMENT: Bottle Name:Guan-fu base Y
COMMENT: PRIME Parent Name:Guan-fu base Y
COMMENT: PRIME in-house No.:V0331
COMMENT: SubCategory_DNP: Terpenoid alkaloids, Diterpene alkaloid, Aconitum alkaloid
CH$NAME: Guanfu base Y
CH$NAME: 11,13,14-trihydroxyhetisan-2-yl acetate
CH$NAME: (1S,3S,16S,19S,10R,14R)-9,10,19-trihydroxy-5-methyl-12-methylene-7-azaheptacyclo(9.6.2.0(1,8).0(5,17).0(7,16).0(9,14).0(14,18))nonadec-3-yl acetate
CH$NAME: Guan-fu base Y
CH$COMPOUND_CLASS: Alkaloids
CH$FORMULA: C22H29NO5
CH$EXACT_MASS: 387.4801
CH$SMILES: C=C1C[C@@]23CC4C5C6(C)C[C@H](OC(C)=O)CC57C2[C@H](O)C1[C@@H](O)[C@]3(O)[C@H]7N4C6
CH$IUPAC: InChI=1S/C22H29NO5/c1-9-4-20-7-12-15-19(3)5-11(28-10(2)24)6-21(15)16(20)14(25)13(9)17(26)22(20,27)18(21)23(12)8-19/h11-18,25-27H,1,4-8H2,2-3H3/t11-,12?,13?,14+,15?,16?,17+,18-,19?,20+,21?,22-/m0/s1
CH$LINK: CAS
110225-59-7
CH$LINK: CHEMSPIDER
20181446
CH$LINK: INCHIKEY
XGTNTUKODZZCGL-FDLOETHHSA-N
AC$INSTRUMENT: Agilent 6410 Triple Quadrupole LC/MS system
AC$INSTRUMENT_TYPE: LC-ESI-QQQ
AC$MASS_SPECTROMETRY: MS_TYPE MS2
AC$MASS_SPECTROMETRY: ION_MODE NEGATIVE
MS$FOCUSED_ION: PRECURSOR_TYPE [M+HCOO]-
PK$SPLASH: splash10-001i-4888980000-160ea65d4f932b0d8ffd
PK$NUM_PEAK: 4299
PK$PEAK: m/z int. rel.int.
50.8 8.2 8
50.9 14.43 14
51.0 20.29 20
51.1 20.5 20
51.2 15.4 15
51.4 9.99 9
51.5 15.06 15
51.6 21.05 21
51.7 22.43 22
51.8 17.32 17
51.9 9.38 9
52.1 7.41 7
52.2 14.65 14
52.3 20.36 20
52.4 19.98 19
52.5 14.49 14
52.7 8.82 8
52.8 13.39 13
52.9 18.48 18
53.0 19.28 19
53.1 15.27 15
53.3 9.53 9
53.4 13.14 13
53.5 18.4 18
53.6 20.91 20
53.7 17.84 17
53.8 10.68 10
54.0 6.51 6
54.1 14.31 14
54.2 22.2 22
54.3 23.71 23
54.4 18.28 18
54.6 9.58 9
54.7 14.24 14
54.8 20.97 20
54.9 23.35 23
55.0 18.66 18
55.1 10.47 10
55.3 7.1 7
55.4 13.53 13
55.5 18.68 18
55.6 17.82 17
55.7 11.38 11
55.9 3.83 3
56.0 10.2 10
56.1 18.67 18
56.2 21.88 21
56.3 17.33 17
56.6 9.88 9
56.7 17.56 17
56.8 22.0 21
56.9 19.18 19
57.0 11.8 11
57.2 7.52 7
57.3 15.15 15
57.4 23.45 23
57.5 25.6 25
57.6 19.65 19
57.7 10.91 10
57.9 10.74 10
58.0 17.85 17
58.1 21.68 21
58.2 19.17 19
58.3 13.13 13
58.5 10.99 10
58.6 16.06 16
58.7 19.33 19
58.8 17.67 17
58.9 12.66 12
59.1 10.31 10
59.2 16.48 16
59.3 23.23 23
59.4 25.32 25
59.5 20.55 20
59.6 11.99 11
59.8 7.42 7
59.9 14.49 14
60.0 20.77 20
60.1 20.55 20
60.2 14.14 14
60.4 5.63 5
60.5 10.41 10
60.6 17.33 17
60.7 20.39 20
60.8 16.95 16
61.1 9.19 9
61.2 16.35 16
61.3 20.99 20
61.4 18.72 18
61.7 10.66 10
61.8 18.78 18
61.9 24.62 24
62.0 22.43 22
62.1 13.57 13
62.3 5.07 5
62.4 12.58 12
62.5 21.64 21
62.6 25.12 25
62.7 21.34 21
62.8 14.97 14
63.0 14.38 14
63.1 19.32 19
63.2 21.8 21
63.3 19.0 18
63.4 12.81 12
63.6 9.0 8
63.7 14.03 14
63.8 18.63 18
63.9 18.79 18
64.0 14.56 14
64.2 9.94 9
64.3 14.64 14
64.4 20.2 20
64.5 21.7 21
64.6 17.61 17
64.7 10.6 10
64.9 7.19 7
65.0 14.95 14
65.1 23.21 23
65.2 24.77 24
65.3 18.16 18
66.2 9.11 9
66.3 17.41 17
66.4 22.77 22
66.5 20.51 20
66.6 12.88 12
66.8 7.39 7
66.9 13.97 13
67.0 20.5 20
67.1 21.28 21
67.2 16.01 15
67.5 10.31 10
67.6 16.59 16
67.7 20.89 20
67.8 19.05 19
67.9 11.85 11
68.1 6.99 6
68.2 15.2 15
68.3 22.61 22
68.4 22.04 22
68.5 14.24 14
68.7 6.23 6
68.8 12.76 12
68.9 20.29 20
69.0 22.34 22
69.1 17.45 17
69.4 10.25 10
69.5 17.38 17
69.6 22.38 22
69.7 21.5 21
69.8 15.84 15
70.0 9.09 9
70.1 13.04 13
70.2 18.03 18
70.3 19.32 19
70.4 15.97 15
70.6 9.75 9
70.7 12.38 12
70.8 17.25 17
70.9 19.73 19
71.0 16.34 16
71.1 9.0 8
71.3 6.61 6
71.4 14.31 14
71.5 20.29 20
71.6 19.48 19
71.7 13.17 13
71.9 8.08 8
72.0 14.18 14
72.1 20.59 20
72.2 21.67 21
72.3 16.47 16
72.5 7.3 7
72.6 11.92 11
72.7 19.37 19
72.8 23.0 22
72.9 19.58 19
73.0 12.3 12
73.2 10.29 10
73.3 17.04 17
73.4 22.01 21
73.5 20.72 20
73.6 13.93 13
73.8 5.32 5
73.9 10.7 10
74.0 18.93 18
74.1 23.13 23
74.2 19.43 19
74.3 11.03 11
74.5 7.99 7
74.6 16.14 16
74.7 23.1 23
74.8 23.8 23
74.9 18.69 18
75.8 11.59 11
75.9 17.29 17
76.0 20.66 20
76.1 18.45 18
76.2 12.34 12
76.4 9.8 9
76.5 17.01 16
76.6 22.94 22
76.7 21.61 21
76.8 13.14 13
77.0 2.26 2
77.1 8.47 8
77.2 17.71 17
77.3 22.66 22
77.4 19.53 19
77.5 11.11 11
77.7 6.76 6
77.8 15.16 15
77.9 22.78 22
78.0 23.37 23
78.1 17.44 17
78.3 9.63 9
78.4 14.84 14
78.5 21.88 21
78.6 24.27 24
78.7 19.67 19
78.8 12.09 12
79.0 10.33 10
79.1 16.89 16
79.2 21.92 21
79.3 20.5 20
79.4 13.06 13
79.6 6.32 6
79.7 13.96 13
79.8 21.83 21
79.9 22.26 22
80.0 14.3 14
80.3 5.69 5
80.4 14.81 14
80.5 20.39 20
80.6 18.38 18
80.7 11.92 11
80.9 10.09 10
81.0 15.53 15
81.1 18.74 18
81.2 16.96 16
81.3 12.14 12
81.5 9.56 9
81.6 14.91 14
81.7 20.95 20
81.8 22.5 22
81.9 17.3 17
82.1 5.79 5
82.2 10.19 10
82.3 19.02 19
82.4 24.87 24
82.5 22.9 22
82.6 14.56 14
82.8 5.0 4
82.9 11.28 11
83.0 19.57 19
83.1 22.3 22
83.2 17.14 17
83.5 9.31 9
83.6 16.66 16
83.7 20.76 20
83.8 18.16 18
83.9 11.44 11
84.1 8.88 8
84.2 15.83 15
84.3 21.32 21
84.4 20.1 20
84.5 13.69 13
84.7 10.04 10
84.8 15.52 15
84.9 20.26 20
85.0 20.81 20
85.1 17.19 17
85.4 11.46 11
85.5 15.92 15
85.6 18.99 18
85.7 17.89 17
85.8 13.65 13
86.0 11.44 11
86.1 16.75 16
86.2 21.71 21
86.3 21.31 21
86.4 15.04 15
86.6 5.9 5
86.7 10.42 10
86.8 16.82 16
86.9 19.04 19
87.0 15.19 15
87.2 7.71 7
87.3 12.46 12
87.4 19.71 19
87.5 22.52 22
87.6 17.38 17
87.9 6.74 6
88.0 16.59 16
88.1 24.84 24
88.2 25.26 25
88.3 18.12 18
88.6 9.61 9
88.7 16.39 16
88.8 19.66 19
88.9 16.59 16
89.0 10.31 10
89.2 7.82 7
89.3 13.89 13
89.4 19.88 19
89.5 20.73 20
89.6 15.4 15
89.8 5.98 5
89.9 10.4 10
90.0 17.91 17
90.1 21.88 21
90.2 18.51 18
90.3 10.32 10
90.5 6.19 6
90.6 14.52 14
90.7 21.99 21
90.8 21.71 21
90.9 13.82 13
91.1 3.19 3
91.2 9.72 9
91.3 19.22 19
91.4 23.46 23
91.5 18.76 18
91.6 9.67 9
91.8 8.69 8
91.9 16.36 16
92.0 20.12 20
92.1 16.75 16
92.2 9.67 9
92.4 7.37 7
92.5 15.2 15
92.6 23.01 22
92.7 24.81 24
92.8 19.88 19
93.6 6.31 6
93.7 10.41 10
93.8 18.23 18
93.9 22.96 22
94.0 20.75 20
94.1 14.06 14
94.3 8.67 8
94.4 13.96 13
94.5 20.56 20
94.6 23.24 23
94.7 19.38 19
94.8 11.79 11
95.0 8.66 8
95.1 15.51 15
95.2 21.22 21
95.3 20.69 20
95.4 14.25 14
95.6 6.64 6
95.7 12.7 12
95.8 20.43 20
95.9 22.6 22
96.0 16.86 16
96.3 8.31 8
96.4 15.93 15
96.5 20.21 20
96.6 17.65 17
96.7 11.1 11
96.9 9.33 9
97.0 16.56 16
97.1 22.34 22
97.2 21.3 21
97.3 13.84 13
97.5 5.32 5
97.6 11.68 11
97.7 19.64 19
97.8 22.06 22
97.9 16.92 16
98.2 8.95 8
98.3 15.83 15
98.4 20.81 20
98.5 20.11 20
98.6 14.23 14
98.8 9.37 9
98.9 16.47 16
99.0 22.71 22
99.1 21.53 21
99.2 13.85 13
99.4 5.11 5
99.5 10.75 10
99.6 19.09 19
99.7 23.64 23
99.8 20.51 20
99.9 12.52 12
100.1 7.92 7
100.2 14.01 13
100.3 18.84 18
100.4 17.88 17
100.5 11.91 11
100.7 7.42 7
100.8 14.23 14
100.9 21.21 21
101.0 22.55 22
101.1 17.65 17
101.4 10.43 10
101.5 16.51 16
101.6 20.86 20
101.7 19.51 19
101.8 13.37 13
102.0 7.62 7
102.1 12.94 12
102.2 18.67 18
102.3 19.45 19
102.4 14.47 14
102.6 6.41 6
102.7 10.58 10
102.8 16.81 16
102.9 19.56 19
103.0 16.55 16
103.2 7.93 7
103.3 11.36 11
103.4 19.14 19
103.5 25.11 25
103.6 24.07 24
103.7 16.42 16
103.9 5.28 5
104.0 10.18 10
104.1 18.36 18
104.2 22.57 22
104.3 19.25 19
104.4 11.99 11
104.6 10.77 10
104.7 17.48 17
104.8 21.71 21
104.9 19.43 19
105.0 12.23 12
105.2 6.39 6
105.3 12.09 12
105.4 18.03 18
105.5 19.09 19
105.6 14.37 14
105.8 6.96 6
105.9 12.76 12
106.0 21.02 20
106.1 24.2 24
106.2 19.34 19
106.3 10.83 10
106.5 7.57 7
106.6 14.13 14
106.7 19.59 19
106.8 19.2 19
106.9 13.02 13
107.1 3.74 3
107.2 7.87 7
107.3 14.64 14
107.4 18.26 18
107.5 15.68 15
107.6 9.34 9
107.8 7.12 7
107.9 12.77 12
108.0 16.7 16
108.1 16.2 16
108.4 13.45 13
108.5 16.39 16
108.6 19.54 19
108.7 21.01 20
108.8 19.13 19
108.9 14.76 14
109.6 8.16 8
109.7 12.39 12
109.8 20.92 20
109.9 26.46 26
110.0 23.35 23
110.1 13.4 13
110.3 3.51 3
110.4 10.04 10
110.5 18.47 18
110.6 22.37 22
110.7 19.02 19
110.8 11.36 11
111.0 7.96 7
111.1 15.44 15
111.2 21.59 21
111.3 21.04 21
111.4 14.82 14
111.6 8.95 8
111.7 14.42 14
111.8 20.32 20
111.9 21.02 20
112.0 15.75 15
112.2 7.27 7
112.3 11.7 11
112.4 18.21 18
112.5 21.04 21
112.6 18.28 18
112.7 13.03 13
112.9 11.07 11
113.0 15.12 15
113.1 18.92 18
113.2 19.34 19
113.3 15.69 15
113.5 9.74 9
113.6 13.86 13
113.7 20.39 20
113.8 23.64 23
113.9 19.98 19
114.0 11.62 11
114.2 7.41 7
114.3 15.71 15
114.4 22.78 22
114.5 21.68 21
114.6 13.15 13
114.8 5.96 5
114.9 14.26 14
115.0 22.91 22
115.1 25.24 25
115.2 20.73 20
115.3 13.9 13
115.5 11.29 11
115.6 15.64 15
115.7 18.32 18
115.8 16.18 16
116.0 9.17 9
116.1 13.06 13
116.2 20.4 20
116.3 25.09 25
116.4 22.34 22
116.5 13.25 13
116.7 3.27 3
116.8 10.19 10
116.9 19.04 19
117.0 22.38 22
117.1 18.27 18
117.2 11.1 11
117.4 9.27 9
117.5 14.56 14
117.6 17.3 17
117.7 14.23 14
118.0 7.08 7
118.1 15.47 15
118.2 22.68 22
118.3 23.04 23
118.4 16.42 16
119.2 7.17 7
119.3 10.57 10
119.4 18.25 18
119.5 23.92 23
119.6 22.3 22
119.7 14.0 13
119.9 5.36 5
120.0 13.13 13
120.1 22.86 22
120.2 26.92 26
120.3 22.91 22
120.4 14.76 14
120.6 9.53 9
120.7 14.75 14
120.8 19.31 19
120.9 18.84 18
121.0 14.11 14
121.2 9.74 9
121.3 14.48 14
121.4 19.88 19
121.5 20.78 20
121.6 15.62 15
121.8 6.83 6
121.9 11.54 11
122.0 18.15 18
122.1 20.47 20
122.2 16.91 16
122.4 9.04 9
122.5 12.32 12
122.6 18.8 18
122.7 22.8 22
122.8 20.12 20
122.9 12.19 12
123.1 6.11 6
123.2 12.94 12
123.3 20.02 19
123.4 21.61 21
123.5 17.12 17
123.7 9.92 9
123.8 14.78 14
123.9 21.3 21
124.0 23.18 23
124.1 18.25 18
124.2 10.18 10
124.4 6.72 6
124.5 13.92 13
124.6 21.05 21
124.7 22.35 22
124.8 16.94 16
125.0 7.01 7
125.1 11.97 11
125.2 20.8 20
125.3 25.92 25
125.4 22.71 22
125.5 14.54 14
125.7 12.46 12
125.8 19.42 19
125.9 23.37 23
126.0 21.04 21
126.1 14.76 14
126.9 8.81 8
127.0 12.2 12
127.1 18.25 18
127.2 22.82 22
127.3 22.17 22
127.4 16.09 16
128.2 4.84 4
128.3 8.86 8
128.4 17.26 17
128.5 23.16 23
128.6 21.92 21
128.7 15.18 15
128.9 9.88 9
129.0 15.15 15
129.1 18.9 18
129.2 16.5 16
129.3 9.85 9
129.5 5.65 5
129.6 11.0 10
129.7 16.46 16
129.8 17.81 17
129.9 14.16 14
130.1 6.57 6
130.2 10.25 10
130.3 17.24 17
130.4 22.14 22
130.5 21.21 21
130.6 15.55 15
130.8 10.83 10
130.9 16.4 16
131.0 21.35 21
131.1 20.36 20
131.2 14.28 14
131.4 8.94 8
131.5 14.01 13
131.6 19.69 19
131.7 21.22 21
131.8 17.28 17
132.1 10.33 10
132.2 16.28 16
132.3 20.38 20
132.4 19.34 19
132.5 14.57 14
132.7 9.93 9
132.8 13.15 13
132.9 16.86 16
133.0 17.19 17
133.1 13.05 13
133.3 6.84 6
133.4 11.6 11
133.5 18.57 18
133.6 21.67 21
133.7 17.47 17
133.8 8.42 8
134.0 2.23 2
134.1 10.35 10
134.2 19.01 18
134.3 21.24 21
134.4 15.91 15
134.7 8.76 8
134.8 15.73 15
134.9 20.48 20
135.0 19.65 19
135.1 14.82 14
135.3 10.25 10
135.4 13.37 13
135.5 16.55 16
135.6 16.4 16
135.7 12.62 12
135.9 7.96 7
136.0 12.53 12
136.1 18.43 18
136.2 20.22 20
136.3 16.09 16
136.6 9.34 9
136.7 16.49 16
136.8 21.71 21
136.9 20.64 20
137.0 14.43 14
137.2 8.65 8
137.3 14.07 14
137.4 20.21 20
137.5 21.48 21
137.6 16.47 16
137.7 9.22 9
137.9 8.25 8
138.0 14.42 14
138.1 18.33 18
138.2 16.2 16
138.3 10.04 10
138.5 7.95 7
138.6 15.26 15
138.7 21.68 21
138.8 21.62 21
138.9 15.25 15
139.1 7.48 7
139.2 13.03 13
139.3 19.85 19
139.4 21.73 21
139.5 17.1 17
139.8 10.22 10
139.9 16.93 16
140.0 21.23 21
140.1 18.89 18
140.2 11.42 11
140.4 7.33 7
140.5 15.82 15
140.6 23.46 23
140.7 23.35 23
140.8 16.05 16
141.0 9.16 9
141.1 16.29 16
141.2 23.52 23
141.3 24.3 24
141.4 17.77 17
141.5 8.8 8
141.7 7.48 7
141.8 15.61 15
141.9 21.54 21
142.0 20.35 20
142.1 13.61 13
142.3 8.42 8
142.4 16.15 16
142.5 24.88 24
142.6 26.78 26
142.7 19.28 19
142.8 8.03 8
143.0 6.34 6
143.1 15.86 15
143.2 21.84 21
143.3 19.29 19
143.4 11.2 11
143.6 5.26 5
143.7 11.41 11
143.8 18.13 18
143.9 20.25 20
144.0 16.6 16
144.9 9.75 9
145.0 15.91 15
145.1 20.76 20
145.2 19.48 19
145.3 12.29 12
145.5 4.86 4
145.6 11.72 11
145.7 19.9 19
145.8 22.42 22
145.9 17.15 17
146.0 8.45 8
146.2 5.51 5
146.3 12.57 12
146.4 17.63 17
146.5 15.94 15
146.8 9.03 9
146.9 17.38 17
147.0 23.7 23
147.1 23.05 23
147.2 16.66 16
147.5 10.35 10
147.6 16.29 16
147.7 20.16 20
147.8 18.39 18
147.9 12.54 12
148.1 10.52 10
148.2 17.11 17
148.3 21.91 21
148.4 19.72 19
148.5 11.62 11
148.7 4.73 4
148.8 11.42 11
148.9 18.38 18
149.0 19.53 19
149.1 14.06 14
149.3 4.71 4
149.4 9.47 9
149.5 17.11 17
149.6 20.72 20
149.7 17.13 17
149.8 9.8 9
150.0 8.15 8
150.1 15.62 15
150.2 22.14 22
150.3 22.65 22
150.4 16.88 16
150.6 7.78 7
150.7 12.72 12
150.8 19.92 19
150.9 22.14 22
151.0 16.64 16
151.1 8.15 8
151.3 6.94 6
151.4 14.48 14
151.5 20.12 20
151.6 19.12 19
151.7 12.41 12
151.9 7.98 7
152.0 15.67 15
152.1 22.88 22
152.2 23.66 23
152.3 17.79 17
152.6 9.7 9
152.7 16.53 16
152.8 21.65 21
152.9 20.81 20
153.0 14.98 14
153.2 9.09 9
153.3 14.47 14
153.4 20.44 20
153.5 20.78 20
153.6 14.32 14
153.8 4.17 4
153.9 9.5 9
154.0 17.66 17
154.1 21.48 21
154.2 17.54 17
154.3 8.95 8
154.5 5.4 5
154.6 14.73 14
154.7 23.57 23
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//
