MassBank Record: MSBNK-RIKEN_NPDepo-NGA03486
ACCESSION: MSBNK-RIKEN_NPDepo-NGA03486
RECORD_TITLE: 9,13-Epoxy-3,18-dihydroxy-15,16-labdanolide; LC-ESI-QQQ; MS2; Frag=135.0V CID@15.0; [M+HCOO]-
DATE: 2018.04.04
AUTHORS: Nogawa T, Okano A, CSRS, RIKEN
LICENSE: CC BY
COMMENT: Origin: Plant
COMMENT: SubCategory_DNP: Diterpenoids, Labdane diterpenoids
CH$NAME: 9,13-Epoxy-3,18-dihydroxy-15,16-labdanolide
CH$COMPOUND_CLASS: Terpenoids
CH$FORMULA: C20H32O5
CH$EXACT_MASS: 352.475
CH$SMILES: C[C@@H]1CCC2[C@](C)(CC[C@H](O)[C@@]2(C)CO)[C@@]12CC1(COC(=O)C1)CO2
CH$IUPAC: InChI=1S/C20H32O5/c1-13-4-5-14-17(2,10-21)15(22)6-7-18(14,3)20(13)9-19(12-25-20)8-16(23)24-11-19/h13-15,21-22H,4-12H2,1-3H3/t13-,14?,15+,17+,18+,19?,20-/m1/s1
CH$LINK: INCHIKEY
QHYFPLAXWXWDJP-GNQMFGHGSA-N
CH$LINK: PUBCHEM
CID:16408478
AC$INSTRUMENT: Agilent 6410 Triple Quadrupole LC/MS system
AC$INSTRUMENT_TYPE: LC-ESI-QQQ
AC$MASS_SPECTROMETRY: MS_TYPE MS2
AC$MASS_SPECTROMETRY: ION_MODE NEGATIVE
MS$FOCUSED_ION: PRECURSOR_TYPE [M+HCOO]-
PK$SPLASH: splash10-0ik9-4888890000-d51d39a1efe3004d2fe5
PK$NUM_PEAK: 4126
PK$PEAK: m/z int. rel.int.
50.8 5.59 5
50.9 10.96 10
51.0 17.89 17
51.1 21.16 21
51.2 18.43 18
51.3 12.44 12
51.5 10.61 10
51.6 15.36 15
51.7 18.51 18
51.8 17.86 17
51.9 14.3 14
52.1 9.69 9
52.2 13.0 12
52.3 17.92 17
52.4 19.97 19
52.5 17.25 17
52.6 12.42 12
52.8 11.0 10
52.9 14.75 14
53.0 17.76 17
53.1 17.53 17
53.2 13.84 13
54.0 7.75 7
54.1 11.02 11
54.2 15.57 15
54.3 17.48 17
54.4 15.42 15
54.5 11.19 11
54.7 9.06 9
54.8 12.88 12
54.9 15.77 15
55.0 14.56 14
55.3 7.96 7
55.4 14.29 14
55.5 21.16 21
55.6 23.41 23
55.7 19.18 19
55.8 11.49 11
56.0 8.02 8
56.1 13.89 13
56.2 17.19 17
56.3 14.23 14
56.6 9.15 9
56.7 13.6 13
56.8 16.15 16
56.9 15.39 15
57.2 10.57 10
57.3 15.04 15
57.4 18.38 18
57.5 16.81 16
57.6 11.43 11
57.8 6.27 6
57.9 10.21 10
58.0 15.5 15
58.1 17.89 17
58.2 15.36 15
58.3 9.8 9
58.5 6.04 6
58.6 10.48 10
58.7 15.56 15
58.8 17.53 17
58.9 15.25 15
59.2 10.44 10
59.3 15.08 15
59.4 18.55 18
59.5 17.39 17
59.6 11.87 11
59.8 6.86 6
59.9 12.94 12
60.0 19.73 19
60.1 21.35 21
60.2 16.67 16
60.5 9.69 9
60.6 15.57 15
60.7 19.67 19
60.8 18.28 18
60.9 12.44 12
61.1 8.68 8
61.2 14.35 14
61.3 19.13 19
61.4 18.72 18
61.5 14.36 14
61.7 11.34 11
61.8 14.59 14
61.9 16.86 16
62.0 16.09 16
62.1 12.94 12
62.3 7.43 7
62.4 9.49 9
62.5 15.17 15
62.6 20.31 20
62.7 19.91 19
62.8 13.57 13
63.0 6.6 6
63.1 13.1 13
63.2 20.14 20
63.3 21.12 21
63.4 15.91 15
63.6 9.89 9
63.7 14.03 14
63.8 17.96 17
63.9 17.44 17
64.0 12.45 12
64.2 5.06 5
64.3 8.24 8
64.4 14.07 14
64.5 18.61 18
64.6 19.09 19
64.7 15.14 15
65.0 7.63 7
65.1 14.69 14
65.2 20.94 20
65.3 20.43 20
65.4 13.58 13
65.6 7.67 7
65.7 14.1 14
65.8 19.85 19
65.9 19.32 19
66.0 13.26 13
66.2 7.47 7
66.3 12.39 12
66.4 17.13 17
66.5 17.11 17
66.6 12.79 12
66.8 8.25 8
66.9 12.26 12
67.0 16.7 16
67.1 17.24 17
67.2 13.4 13
67.4 9.35 9
67.5 14.09 14
67.6 19.48 19
67.7 20.66 20
67.8 16.26 16
68.1 10.28 10
68.2 16.32 16
68.3 20.08 20
68.4 18.72 18
68.5 13.4 13
68.8 8.97 8
68.9 14.38 14
69.0 18.15 18
69.1 17.7 17
70.0 10.09 10
70.1 14.61 14
70.2 18.96 18
70.3 19.71 19
70.4 15.82 15
70.7 9.98 9
70.8 14.9 14
70.9 17.51 17
71.0 15.77 15
71.3 11.67 11
71.4 15.1 15
71.5 16.79 16
71.6 14.93 14
71.7 10.67 10
71.9 7.32 7
72.0 10.94 10
72.1 14.81 14
72.2 15.36 15
72.3 12.27 12
72.5 7.41 7
72.6 10.31 10
72.7 15.95 15
72.8 20.81 20
72.9 20.72 20
73.0 14.81 14
73.2 6.11 6
73.3 11.38 11
73.4 17.97 17
73.5 19.21 19
73.6 14.2 14
73.8 6.95 6
73.9 11.35 11
74.0 16.76 16
74.1 18.12 18
74.2 14.47 14
74.3 9.2 9
74.5 8.25 8
74.6 12.58 12
74.7 16.15 16
74.8 16.41 16
74.9 13.14 13
75.2 8.18 8
75.3 13.13 13
75.4 17.45 17
75.5 17.67 17
75.6 14.3 14
75.8 11.9 11
75.9 14.72 14
76.0 16.44 16
76.1 15.42 15
76.2 12.39 12
76.4 9.31 9
76.5 12.5 12
76.6 16.66 16
76.7 17.76 17
76.8 14.24 14
77.0 7.18 7
77.1 10.33 10
77.2 15.82 15
77.3 18.81 18
77.4 16.93 16
77.5 12.07 12
77.7 9.5 9
77.8 14.23 14
77.9 18.52 18
78.0 18.2 18
78.1 13.48 13
78.3 10.06 10
78.4 15.45 15
78.5 20.6 20
78.6 21.29 21
78.7 17.22 17
78.8 11.61 11
79.0 9.14 9
79.1 12.97 12
79.2 16.79 16
79.3 17.48 17
79.4 14.56 14
79.6 9.57 9
79.7 12.32 12
79.8 16.29 16
79.9 17.54 17
80.0 14.35 14
80.3 8.92 8
80.4 14.3 14
80.5 17.5 17
80.6 15.65 15
80.7 10.28 10
80.9 5.94 5
81.0 10.83 10
81.1 16.63 16
81.2 18.6 18
81.3 15.05 15
81.5 6.94 6
81.6 10.42 10
81.7 17.02 17
81.8 20.95 20
81.9 19.09 19
82.0 13.28 13
82.2 8.27 8
82.3 11.77 11
82.4 15.51 15
82.5 16.46 16
82.6 14.24 14
82.8 9.9 9
82.9 12.22 12
83.0 16.05 16
83.1 17.89 17
83.2 16.11 16
83.3 12.52 12
83.5 11.37 11
83.6 14.56 14
83.7 17.25 17
83.8 17.22 17
83.9 14.47 14
84.1 10.96 10
84.2 14.0 13
84.3 18.2 18
84.4 19.58 19
84.5 16.37 16
85.4 1.97 1
85.5 10.31 10
85.6 18.29 18
85.7 20.31 20
85.8 15.85 15
86.7 9.23 9
86.8 15.19 15
86.9 20.29 20
87.0 20.48 20
87.1 15.66 15
87.3 8.04 8
87.4 11.48 11
87.5 16.67 16
87.6 18.43 18
87.7 14.99 14
88.0 10.27 10
88.1 16.2 16
88.2 19.47 19
88.3 17.71 17
89.2 3.74 3
89.3 11.03 11
89.4 19.91 19
89.5 23.78 23
89.6 19.42 19
89.7 9.96 9
89.9 4.34 4
90.0 11.83 11
90.1 18.0 17
90.2 17.65 17
90.3 12.61 12
90.5 10.33 10
90.6 14.98 14
90.7 17.77 17
90.8 15.54 15
90.9 10.09 10
91.1 7.27 7
91.2 12.35 12
91.3 17.27 17
91.4 18.12 18
91.5 14.67 14
91.7 9.21 9
91.8 12.35 12
91.9 18.02 18
92.0 22.57 22
92.1 22.69 22
92.2 17.92 17
92.5 11.03 11
92.6 16.76 16
92.7 20.81 20
92.8 19.59 19
92.9 14.18 14
93.1 9.38 9
93.2 13.69 13
93.3 18.08 18
93.4 18.23 18
93.5 13.84 13
93.7 8.65 8
93.8 13.48 13
93.9 19.44 19
94.0 20.86 20
94.1 15.77 15
94.4 8.4 8
94.5 15.13 15
94.6 19.28 19
94.7 18.06 18
94.8 13.03 13
95.0 9.0 8
95.1 14.49 14
95.2 20.31 20
95.3 21.01 20
95.4 15.97 15
95.6 8.66 8
95.7 12.93 12
95.8 18.55 18
95.9 19.88 19
96.0 15.57 15
96.9 8.27 8
97.0 14.61 14
97.1 19.97 19
97.2 19.82 19
97.3 14.15 14
97.6 6.69 6
97.7 14.03 14
97.8 19.64 19
97.9 19.04 19
98.8 10.41 10
98.9 14.46 14
99.0 16.05 16
99.1 14.15 14
99.2 10.61 10
99.4 6.37 6
99.5 8.99 8
99.6 14.52 14
99.7 19.1 19
99.8 18.69 18
99.9 13.49 13
100.1 7.66 7
100.2 11.92 11
100.3 16.72 16
100.4 17.56 17
100.5 14.09 14
100.7 9.2 9
100.8 12.06 12
100.9 15.62 15
101.0 16.96 16
101.1 15.43 15
101.2 12.16 12
101.4 9.52 9
101.5 12.88 12
101.6 16.14 16
101.7 15.2 15
101.8 9.78 9
102.0 3.9 3
102.1 9.25 9
102.2 16.43 16
102.3 20.32 20
102.4 18.6 18
102.5 13.54 13
102.7 11.64 11
102.8 15.77 15
102.9 18.25 18
103.0 16.72 16
103.1 12.79 12
103.3 10.38 10
103.4 14.87 14
103.5 20.06 20
103.6 21.44 21
103.7 17.45 17
103.8 11.22 11
104.0 7.06 7
104.1 10.45 10
104.2 14.04 14
104.3 14.32 14
104.4 10.76 10
104.6 7.4 7
104.7 11.6 11
104.8 15.63 15
104.9 16.18 16
105.0 13.2 13
105.2 8.4 8
105.3 11.37 11
105.4 16.23 16
105.5 18.84 18
105.6 17.28 17
105.9 13.58 13
106.0 16.43 16
106.1 17.7 17
106.2 16.34 16
106.3 13.2 13
106.5 10.18 10
106.6 13.16 13
106.7 17.47 17
106.8 19.83 19
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107.0 13.23 13
107.2 9.49 9
107.3 12.73 12
107.4 14.96 14
107.5 13.29 13
107.8 7.32 7
107.9 12.41 12
108.0 17.36 17
108.1 18.25 18
108.2 14.78 14
108.4 9.75 9
108.5 13.55 13
108.6 18.64 18
108.7 20.32 20
108.8 16.67 16
108.9 10.19 10
109.1 6.65 6
109.2 12.52 12
109.3 18.52 18
109.4 19.61 19
109.5 15.37 15
110.3 6.07 6
110.4 10.62 10
110.5 19.91 19
110.6 28.85 28
110.7 31.72 31
110.8 26.44 26
110.9 17.7 17
111.1 14.88 14
111.2 19.51 19
111.3 21.03 21
111.4 17.36 17
111.5 11.52 11
111.7 10.54 10
111.8 14.84 14
111.9 16.64 16
112.0 14.3 14
112.2 9.47 9
112.3 12.64 12
112.4 16.99 16
112.5 18.12 18
112.6 14.27 14
112.7 7.82 7
112.9 4.74 4
113.0 11.37 11
113.1 18.95 18
113.2 21.93 21
113.3 18.44 18
113.4 12.15 12
113.6 11.25 11
113.7 16.09 16
113.8 18.92 18
113.9 17.42 17
114.0 12.71 12
114.2 7.47 7
114.3 11.08 11
114.4 16.11 16
114.5 18.49 18
114.6 16.61 16
115.5 9.93 9
115.6 14.98 14
115.7 17.63 17
115.8 14.73 14
116.1 8.42 8
116.2 15.01 14
116.3 20.81 20
116.4 22.13 22
116.5 18.58 18
117.4 8.21 8
117.5 14.93 14
117.6 19.93 19
117.7 18.93 18
117.8 12.96 12
118.0 6.25 6
118.1 10.45 10
118.2 15.86 15
118.3 17.3 17
118.4 12.82 12
118.6 3.16 3
118.7 7.46 7
118.8 15.48 15
118.9 21.13 21
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120.6 8.28 8
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121.0 15.31 15
121.8 6.31 6
121.9 10.3 10
122.0 17.5 17
122.1 21.96 21
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122.3 13.8 13
122.5 9.26 9
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123.9 19.79 19
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125.3 19.45 19
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125.5 11.37 11
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130.3 15.42 15
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130.6 10.77 10
130.8 7.64 7
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131.9 11.35 11
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132.3 12.0 11
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132.5 14.67 14
132.6 11.81 11
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133.1 16.27 16
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133.5 16.03 16
133.6 20.05 20
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133.8 13.42 13
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134.2 19.36 19
134.3 21.3 21
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140.7 21.82 21
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150.6 7.41 7
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153.5 18.08 18
153.6 14.2 14
153.7 7.76 7
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154.1 18.26 18
154.2 18.73 18
154.3 14.85 14
154.5 11.34 11
154.6 15.48 15
154.7 20.09 20
154.8 21.19 21
154.9 17.45 17
155.8 8.76 8
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156.0 20.08 20
156.1 19.21 19
156.2 13.57 13
156.4 6.92 6
156.5 11.46 11
156.6 17.65 17
156.7 20.37 20
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157.1 9.17 9
157.2 14.93 14
157.3 19.53 19
157.4 18.28 18
157.5 11.95 11
157.7 6.05 6
157.8 11.11 11
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158.6 19.53 19
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159.3 14.39 14
159.4 10.99 10
159.6 6.39 6
159.7 10.44 10
159.8 16.79 16
159.9 20.45 20
160.0 18.17 18
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160.3 10.06 10
160.4 15.72 15
160.5 19.64 19
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160.7 14.36 14
160.9 10.77 10
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161.1 16.4 16
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161.3 14.59 14
161.4 10.91 10
161.6 9.06 9
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161.8 15.28 15
161.9 15.6 15
162.0 13.16 13
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162.4 17.86 17
162.5 16.84 16
162.6 11.58 11
162.8 6.83 6
162.9 11.32 11
163.0 16.44 16
163.1 18.63 18
163.2 16.86 16
163.3 12.64 12
163.5 10.31 10
163.6 14.5 14
163.7 18.2 18
163.8 17.82 17
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//
