ACCESSION: MSBNK-Waters-WA001532
RECORD_TITLE: Glipizide; LC-ESI-Q; MS; POS; 60 V
DATE: 2016.01.19 (Created 2007.08.01, modified 2011.05.06)
AUTHORS: Nihon Waters K.K.
LICENSE: CC BY-NC

CH$NAME: Glipizide
CH$COMPOUND_CLASS: N/A
CH$FORMULA: C₂₁H₂₇N₅O₄S
CH$EXACT_MASS: 445.17838
CH$SMILES: Cc(c3)ncc(n3)C(=O)NCCc(c2)ccc(c2)S(=O)(=O)NC(=O)NC(C1)CCCC1
CH$IUPAC: InChI=1S/C21H27N5O4S/c1-15-13-24-19(14-23-15)20(27)22-12-11-16-7-9-18(10-8-16)31(29,30)26-21(28)25-17-5-3-2-4-6-17/h7-10,13-14,17H,2-6,11-12H2,1H3,(H,22,27)(H2,25,26,28)
CH$LINK: CAS 29094-61-9
CH$LINK: INCHIKEY ZJJXGWJIGJFDTL-UHFFFAOYSA-N
CH$LINK: COMPTOX DTXSID0040676

AC$INSTRUMENT: ZQ, Waters
AC$INSTRUMENT_TYPE: LC-ESI-Q
AC$MASS_SPECTROMETRY: MS_TYPE MS
AC$MASS_SPECTROMETRY: ION_MODE POSITIVE
AC$MASS_SPECTROMETRY: IONIZATION ESI
AC$CHROMATOGRAPHY: RETENTION_TIME 15.820 min
AC$CHROMATOGRAPHY: COLUMN_NAME 2.1 mm id - 3. 5{mu}m XTerra C18MS
AC$CHROMATOGRAPHY: COLUMN_TEMPERATURE 35 C
AC$CHROMATOGRAPHY: SAMPLING_CONE 60 V

MS$DATA_PROCESSING: FIND_PEAK ignore rel.int. < 5

PK$SPLASH: splash10-0v4r-0934100000-02bbe81e952940907c1c
PK$NUM_PEAK: 118
PK$PEAK: m/z int. rel.int.
  100 274 274
  101 16 16
  103 513 513
  104 51 51
  107 67 67
  109 8 8
  111 71 71
  118 12 12
  119 31 31
  120 255 255
  121 376 376
  122 71 71
  123 24 24
  124 12 12
  127 8 8
  131 325 325
  132 24 24
  134 24 24
  136 12 12
  138 20 20
  139 94 94
  144 51 51
  145 8 8
  148 94 94
  149 51 51
  150 286 286
  151 31 31
  152 12 12
  153 8 8
  155 16 16
  166 47 47
  167 999 999
  168 86 86
  169 59 59
  175 8 8
  177 8 8
  179 8 8
  181 8 8
  183 12 12
  184 63 63
  185 16 16
  191 8 8
  197 8 8
  198 16 16
  201 12 12
  203 43 43
  204 8 8
  210 12 12
  211 51 51
  212 8 8
  220 20 20
  222 98 98
  223 12 12
  225 8 8
  226 12 12
  228 8 8
  238 35 35
  240 94 94
  241 12 12
  246 31 31
  247 8 8
  255 16 16
  256 141 141
  257 12 12
  258 67 67
  259 8 8
  268 12 12
  286 846 846
  287 149 149
  288 51 51
  289 8 8
  303 8 8
  304 372 372
  305 59 59
  306 20 20
  319 16 16
  321 690 690
  322 129 129
  323 47 47
  324 8 8
  343 47 47
  344 8 8
  345 20 20
  347 168 168
  348 27 27
  349 31 31
  353 8 8
  369 219 219
  370 35 35
  371 16 16
  385 114 114
  386 16 16
  387 16 16
  401 31 31
  402 8 8
  427 24 24
  428 8 8
  429 20 20
  430 8 8
  444 63 63
  445 8 8
  446 121 121
  447 24 24
  448 8 8
  452 20 20
  453 8 8
  460 8 8
  462 8 8
  466 8 8
  468 227 227
  469 47 47
  470 16 16
  484 145 145
  485 31 31
  486 20 20
  487 8 8
  490 8 8
  500 12 12
//