MassBank Record: CA000088



 Deoxymyxol 2'-(2,4-di-O-methyl-fucoside); FAB-EBEB; MS2; m/z: 742.52; [M]+* 
Mass Spectrum
Chemical Structure
Generated by the Chemistry Development Kit (http://github.com/cdk) \n

ACCESSION: CA000088
RECORD_TITLE: Deoxymyxol 2'-(2,4-di-O-methyl-fucoside); FAB-EBEB; MS2; m/z: 742.52; [M]+*
DATE: 2016.01.19 (Created 2010.04.01, modified 2011.05.10)
AUTHORS: Akimoto N, Graduate School of Pharmaceutical Sciences, Kyoto University and Maoka T, Research Institute for Production Development
LICENSE: CC BY-SA
PUBLICATION: Shinichi Takaichi, Takashi Maoka and Kazumori Masamtoto, Myxoxanthophyll in Synechocystis sp. PCC 6803 is Myxol 2'-Dimethyl-Fucoside, (3R,2'S)-Myxol 2'-(2,4-di-O-Methyl-?-L-Fucoside), not Rhamnoside, Plant Cell Physiol, 42, 756-762 (2001).
COMMENT: Profile spectrum of this record is given as a JPEG file.
COMMENT: [Profile] CA000088.jpg

CH$NAME: Deoxymyxol 2'-(2,4-di-O-methyl-fucoside) CH$COMPOUND_CLASS: N/A CH$FORMULA: C48H70O6 CH$EXACT_MASS: 742.51724 CH$SMILES: C(C=CC=C(C)C=CC=C(C=CC(C(C)(C)O)OC(C(OC)2)OC(C)C(OC)C2O)C)(C)=CC=CC=C(C=CC=C(C)C=CC(C1(C)C)=C(C)CCC1)C CH$IUPAC: InChI=1S/C48H70O6/c1-34(20-14-15-21-35(2)23-17-26-37(4)29-31-41-39(6)28-19-33-47(41,8)9)22-16-24-36(3)25-18-27-38(5)30-32-42(48(10,11)50)54-46-45(52-13)43(49)44(51-12)40(7)53-46/h14-18,20-27,29-32,40,42-46,49-50H,19,28,33H2,1-13H3/b15-14+,22-16+,23-17+,25-18+,31-29+,32-30+,34-20+,35-21+,36-24+,37-26+,38-27+/t40?,42-,43?,44?,45?,46?/m0/s1
AC$INSTRUMENT: JMS-HX/HX 110A, JEOL AC$INSTRUMENT_TYPE: FAB-EBEB AC$MASS_SPECTROMETRY: MS_TYPE MS2 AC$MASS_SPECTROMETRY: ION_MODE POSITIVE AC$MASS_SPECTROMETRY: ATOM_GUN_CURRENT 5 mA AC$MASS_SPECTROMETRY: BOMBARDMENT 6 kV xenon AC$MASS_SPECTROMETRY: COLLISION_ENERGY 3 kV AC$MASS_SPECTROMETRY: COLLISION_GAS Ar AC$MASS_SPECTROMETRY: GAS_PRESSURE adjust to attenuate the intensity of the precursor ion by 30 % AC$MASS_SPECTROMETRY: IONIZATION FAB AC$MASS_SPECTROMETRY: MATRIX 1-2 uL m-NBA AC$MASS_SPECTROMETRY: PROBE_TIP stainless-steel
MS$FOCUSED_ION: BASE_PEAK 73.0738 MS$FOCUSED_ION: PRECURSOR_M/Z 742.52 MS$FOCUSED_ION: PRECURSOR_TYPE [M]+* MS$DATA_PROCESSING: RELATIVE_M/Z normalised by peak(m/z=73.0738). set 999 for peak(m/z=742.7093,rel=6675).
PK$SPLASH: splash10-0006-6910011600-c56d54e744306679833f PK$NUM_PEAK: 923 PK$PEAK: m/z int. rel.int. 0.5449 0.01 1 1.3953 0.03 2 2.2512 0.01 1 5.8750 0.02 1 7.1814 0.01 1 14.0240 0.02 1 15.0215 0.10 7 15.8863 0.01 1 18.1039 0.02 1 18.9908 0.01 1 22.3941 0.04 3 22.9996 0.10 7 25.0096 0.01 1 25.3708 0.01 1 26.0158 0.05 3 27.0214 0.34 23 28.0310 0.05 3 29.0259 0.43 29 29.9856 0.02 1 31.0248 0.13 9 31.4797 0.01 1 33.0306 0.47 31 33.3879 0.01 1 37.0072 0.01 1 37.9746 0.04 3 39.0257 0.59 39 40.0467 0.13 9 40.6854 0.01 1 41.0441 1.88 126 41.6269 0.01 1 42.0343 0.08 5 43.0352 1.89 126 44.0156 0.05 3 45.0402 2.37 158 47.0416 0.03 2 49.0315 0.01 1 50.0299 0.09 6 50.6992 0.02 1 51.0267 0.48 32 52.0313 0.10 7 53.0422 0.94 63 54.0538 0.12 8 55.0574 2.93 196 56.0416 0.11 7 57.0524 1.39 93 57.5812 0.01 1 58.0674 0.09 6 59.0608 8.44 564 59.6885 0.03 2 60.0363 0.21 14 61.0383 0.32 21 62.0323 0.07 5 63.0341 0.30 20 63.4373 0.02 1 64.0359 0.08 5 65.0473 0.52 35 66.0529 0.20 13 66.5056 0.01 1 67.0631 1.09 73 67.9987 0.05 3 69.0742 3.97 265 70.0629 0.08 5 70.5429 0.02 1 71.0601 3.66 244 72.0657 1.07 71 73.0738 14.96 999 74.0263 0.38 25 74.4541 0.02 1 75.0557 7.46 498 75.4790 0.04 3 76.0582 0.14 9 77.0489 2.02 135 77.5170 0.03 2 78.0571 0.52 35 78.4880 0.03 2 79.0671 2.16 144 80.0604 0.23 15 80.4927 0.01 1 81.0836 2.95 197 81.6208 0.01 1 82.0490 0.25 17 83.0614 2.18 146 84.0518 0.04 3 84.4865 0.01 1 85.0484 3.80 254 86.0877 0.03 2 87.0538 4.74 317 88.0273 0.15 10 89.0693 6.44 430 90.0597 0.10 7 91.0658 4.93 329 92.0632 0.46 31 93.0828 3.05 204 94.0807 0.31 21 95.0991 3.52 235 96.0990 0.04 3 97.0882 2.55 170 98.0749 0.15 10 99.0656 13.69 914 99.9870 0.06 4 100.4435 0.02 1 101.0854 9.05 604 102.0906 0.93 62 102.5211 0.03 2 103.0848 3.16 211 103.6874 0.01 1 104.0862 0.27 18 105.0981 7.16 478 106.1072 0.36 24 107.1118 2.66 178 108.0850 0.13 9 109.1206 1.53 102 110.0590 0.03 2 111.0802 2.54 170 111.8990 0.06 4 112.1491 0.03 2 113.0880 0.71 47 114.1047 0.22 15 115.0979 5.89 393 116.0997 0.74 49 117.0897 2.63 176 117.7030 0.03 2 118.1122 0.46 31 119.1109 6.76 451 120.1062 0.50 33 120.6217 0.02 1 121.1170 2.52 168 121.5578 0.03 2 122.1381 0.14 9 123.1403 0.83 55 124.0855 0.07 5 125.0788 2.80 187 126.1411 0.16 11 127.0857 0.98 65 128.0768 2.91 194 129.0920 4.54 303 130.0793 1.18 79 131.0906 7.05 471 132.1034 0.66 44 133.1107 4.09 273 134.1090 0.38 25 135.1263 0.72 48 136.0485 0.14 9 137.1283 0.76 51 138.0407 0.05 3 138.3715 0.03 2 139.0476 0.37 25 139.5533 0.02 1 140.1000 0.13 9 140.4494 0.05 3 141.0903 2.24 150 141.5496 0.04 3 142.0924 2.20 147 143.0834 11.39 761 144.1006 1.56 104 145.1049 4.91 328 146.1053 0.35 23 146.5624 0.06 4 147.1141 1.40 93 148.0581 0.14 9 149.1192 0.32 21 150.0601 0.09 6 151.1344 0.10 7 152.0686 0.85 57 153.0880 1.25 83 154.1157 0.56 37 155.1123 2.48 166 156.1064 1.62 108 157.1033 8.56 572 158.1320 0.82 55 159.1257 2.71 181 160.1024 0.25 17 161.1433 1.41 94 161.6624 0.02 1 162.1564 0.15 10 163.1669 0.34 23 164.1150 0.12 8 165.1111 1.86 124 166.1155 0.59 39 166.6371 0.08 5 167.1227 1.51 101 168.1126 0.85 57 168.5678 0.05 3 169.1454 2.85 190 170.1536 0.92 61 170.4893 0.07 5 171.1555 2.21 148 172.1364 0.29 19 172.7158 0.08 5 173.1712 1.26 84 174.1611 0.26 17 175.1557 6.47 432 176.1437 0.27 18 176.4940 0.07 5 177.1968 0.81 54 178.1517 1.22 81 179.1680 1.45 97 180.1705 0.58 39 180.6433 0.04 3 181.1775 1.70 114 181.7174 0.02 1 182.1840 0.69 46 183.1785 2.35 157 184.1628 0.49 33 185.2030 1.39 93 186.0248 0.11 7 186.5724 0.02 1 187.1958 0.75 50 187.7198 0.03 2 188.2274 0.10 7 189.1472 0.59 39 190.1268 0.25 17 191.1238 0.64 43 191.6197 0.03 2 192.1455 0.66 44 193.1421 1.47 98 194.1320 0.82 55 194.6217 0.03 2 195.1653 2.17 145 196.1548 0.62 41 196.6581 0.04 3 197.1654 2.13 142 198.1377 0.22 15 199.1739 0.74 49 200.1773 0.34 23 201.1683 0.51 34 202.0892 0.47 31 203.1711 0.87 58 204.1249 0.24 16 205.1391 0.62 41 206.1017 0.46 31 207.1639 1.44 96 208.1408 0.46 31 208.5527 0.08 5 209.1726 1.91 128 210.2032 0.32 21 211.1763 0.94 63 212.1894 0.22 15 213.1618 0.48 32 213.7440 0.04 3 214.3001 0.09 6 215.1459 0.53 35 215.6234 0.09 6 216.1237 0.22 15 216.6524 0.04 3 217.1304 0.40 27 217.5728 0.05 3 218.2017 0.22 15 219.1775 0.67 45 220.1614 0.30 20 221.1667 0.98 65 222.1460 0.25 17 222.7123 0.03 2 223.2014 0.65 43 224.1819 0.27 18 224.5939 0.02 1 225.1893 0.46 31 226.1992 0.23 15 227.2248 0.44 29 227.6223 0.05 3 228.1619 0.19 13 228.5539 0.06 4 229.1677 0.37 25 230.1873 0.19 13 231.2036 0.44 29 232.2034 0.34 23 233.1771 0.63 42 234.1892 0.22 15 235.1886 0.84 56 236.2683 0.19 13 237.2212 0.53 35 238.2544 0.19 13 239.1967 0.38 25 239.5890 0.10 7 240.2176 0.16 11 241.2160 0.65 43 241.7117 0.02 1 242.2188 0.21 14 242.6631 0.02 1 243.2640 0.52 35 244.1589 0.16 11 245.2070 0.51 34 245.6786 0.05 3 246.2307 0.19 13 247.1937 0.50 33 248.2604 0.14 9 249.2496 0.38 25 250.2593 0.16 11 250.7290 0.02 1 251.3038 0.33 22 252.1730 0.16 11 253.2605 0.43 29 254.2164 0.16 11 255.2321 0.36 24 256.2845 0.23 15 257.2092 0.28 19 257.7051 0.04 3 258.1648 0.11 7 259.1860 0.28 19 260.2382 0.14 9 261.2449 0.32 21 262.3095 0.13 9 263.2364 0.27 18 263.7719 0.03 2 264.2519 0.10 7 265.2736 0.24 16 265.7231 0.04 3 266.2784 0.16 11 267.1913 0.53 35 268.2815 0.18 12 268.6642 0.03 2 269.2894 0.49 33 270.1725 0.14 9 271.2273 0.26 17 272.2806 0.15 10 272.7929 0.01 1 273.3324 0.17 11 274.2554 0.13 9 275.2558 0.32 21 275.8112 0.23 15 276.1776 0.09 6 276.6154 0.02 1 277.2424 0.12 8 278.3401 0.12 8 279.3185 0.16 11 279.7740 0.03 2 280.2296 0.10 7 281.2607 0.22 15 282.2768 0.15 10 283.2642 0.29 19 284.2442 0.18 12 284.7141 0.02 1 285.2903 0.17 11 286.1898 0.08 5 286.5980 0.02 1 287.2539 0.18 12 288.1733 0.09 6 288.6960 0.01 1 289.2517 0.16 11 290.2879 0.07 5 290.6366 0.01 1 291.3070 0.22 15 292.2237 0.09 6 293.2763 0.33 22 294.2847 0.16 11 295.2352 0.07 5 295.7863 0.01 1 296.3490 0.08 5 297.1720 0.11 7 297.4069 0.05 3 297.8222 0.02 1 298.3416 0.09 6 299.3147 0.12 8 299.8692 0.02 1 300.1755 0.04 3 301.3043 0.08 5 302.3307 0.10 7 303.3651 0.13 9 304.3687 0.05 3 305.3707 0.28 19 306.2700 0.06 4 307.2939 0.13 9 308.3045 0.05 3 309.3367 0.09 6 310.4160 0.03 2 311.3574 0.06 4 312.0267 0.04 3 313.2546 0.09 6 314.2630 0.11 7 315.2775 0.09 6 316.2761 0.07 5 316.8831 0.04 3 317.3072 0.08 5 318.2938 0.10 7 319.3079 0.23 15 320.3048 0.18 12 321.2843 0.15 10 321.6817 0.08 5 322.2836 0.09 6 323.3085 0.10 7 323.5930 0.04 3 324.0160 0.02 1 324.3474 0.07 5 324.7158 0.04 3 325.4527 0.06 4 326.3712 0.06 4 326.7417 0.02 1 327.2703 0.06 4 328.2945 0.06 4 328.9365 0.03 2 329.3619 0.10 7 330.1641 0.10 7 330.7439 0.03 2 331.3472 0.22 15 331.7768 0.02 1 332.3392 0.04 3 332.8900 0.06 4 333.4194 0.13 9 334.3045 0.14 9 334.6640 0.03 2 335.3969 0.25 17 335.8914 0.01 1 336.4328 0.03 2 337.1562 0.03 2 338.2415 0.05 3 338.5721 0.02 1 339.2449 0.09 6 339.8866 0.02 1 341.4912 0.05 3 342.3015 0.04 3 343.3685 0.10 7 344.3144 0.02 1 344.7726 0.03 2 345.3152 0.11 7 345.6992 0.04 3 346.2595 0.22 15 346.6063 0.05 3 347.3156 0.13 9 348.3544 0.06 4 349.2639 0.06 4 349.6267 0.02 1 350.0796 0.01 1 350.4796 0.02 1 351.2975 0.09 6 352.2469 0.01 1 353.3475 0.08 5 354.4641 0.03 2 355.3023 0.12 8 355.7852 0.02 1 356.1229 0.05 3 356.4429 0.06 4 357.1949 0.08 5 357.4542 0.04 3 358.3930 0.08 5 359.3968 0.12 8 360.3851 0.15 10 361.3815 0.05 3 362.2306 0.07 5 363.3591 0.03 2 364.2774 0.13 9 366.3333 0.04 3 367.3817 0.04 3 368.3518 0.05 3 369.2180 0.05 3 369.9370 0.01 1 370.4104 0.06 4 371.3791 0.13 9 372.3892 0.10 7 373.3661 0.06 4 373.6178 0.04 3 373.9598 0.01 1 374.4691 0.09 6 375.3362 0.02 1 375.8908 0.04 3 376.3470 0.02 1 377.3994 0.04 3 377.8539 0.01 1 378.2316 0.04 3 378.5110 0.01 1 379.3414 0.04 3 380.4317 0.04 3 381.2939 0.06 4 381.6364 0.01 1 382.6917 0.04 3 383.4144 0.06 4 384.4070 0.07 5 385.3979 0.20 13 386.4736 0.13 9 387.5219 0.09 6 387.8392 0.04 3 388.4994 0.14 9 389.3253 0.01 1 390.3130 0.05 3 390.8690 0.02 1 391.3778 0.15 10 392.3382 0.07 5 393.3481 0.02 1 394.0918 0.04 3 394.5377 0.02 1 394.9481 0.04 3 395.3308 0.03 2 396.4764 0.08 5 397.3618 0.13 9 398.5137 0.03 2 398.8589 0.04 3 399.4685 0.11 7 400.4472 0.10 7 401.3707 0.05 3 401.8463 0.02 1 402.4443 0.08 5 402.8391 0.02 1 403.3741 0.11 7 404.2072 0.07 5 404.6949 0.05 3 405.3504 0.02 1 405.9211 0.05 3 406.3300 0.02 1 407.3116 0.05 3 409.1390 0.05 3 409.7970 0.02 1 410.8088 0.04 3 411.0953 0.02 1 411.4883 0.11 7 411.8041 0.04 3 412.1475 0.06 4 412.5482 0.15 10 413.4148 0.06 4 414.5856 0.09 6 415.3734 0.09 6 416.0824 0.06 4 416.4873 0.13 9 417.4729 0.49 33 418.0932 0.06 4 418.5002 0.08 5 419.5256 0.01 1 420.4109 0.04 3 421.4030 0.05 3 421.9307 0.03 2 422.4485 0.04 3 423.1345 0.02 1 423.5200 0.03 2 424.0281 0.05 3 424.4592 0.10 7 425.5922 0.07 5 426.3773 0.04 3 426.8758 0.01 1 427.6868 0.02 1 428.4266 0.07 5 429.3684 0.11 7 430.4230 0.14 9 430.9019 0.02 1 431.1948 0.02 1 431.8559 0.03 2 432.2458 0.04 3 432.4972 0.04 3 433.3226 0.05 3 434.4155 0.07 5 435.6471 0.02 1 435.9600 0.04 3 436.5164 0.02 1 437.3364 0.08 5 438.3307 0.07 5 439.2202 0.01 1 440.4506 0.03 2 441.3859 0.02 1 442.4660 0.08 5 443.4630 0.11 7 444.2341 0.02 1 444.5592 0.03 2 444.8189 0.01 1 445.5069 0.04 3 447.7070 0.01 1 448.4848 0.06 4 449.4151 0.05 3 450.5593 0.03 2 451.2285 0.03 2 451.6384 0.05 3 452.6700 0.04 3 453.1651 0.07 5 453.6839 0.04 3 454.5950 0.01 1 455.5438 0.06 4 456.7859 0.02 1 457.3387 0.04 3 457.6933 0.04 3 458.3116 0.05 3 460.4221 0.07 5 461.3339 0.05 3 461.6610 0.04 3 462.4123 0.04 3 464.1452 0.04 3 464.7499 0.04 3 465.2358 0.03 2 465.6185 0.06 4 466.3660 0.04 3 466.6453 0.03 2 467.6080 0.01 1 468.6223 0.04 3 470.3620 0.06 4 470.9467 0.03 2 471.4500 0.05 3 472.4568 0.07 5 473.3845 0.10 7 473.8444 0.02 1 474.4173 0.04 3 475.0518 0.04 3 475.5573 0.03 2 476.5666 0.06 4 476.8660 0.02 1 477.3519 0.07 5 477.7703 0.04 3 478.4763 0.24 16 478.8393 0.09 6 479.6387 0.09 6 480.1941 0.04 3 480.6543 0.07 5 481.3764 0.02 1 482.4835 0.12 8 483.4776 0.05 3 483.9559 0.03 2 486.5558 0.09 6 487.0005 0.06 4 487.3598 0.08 5 487.7469 0.02 1 488.3504 0.04 3 488.9282 0.06 4 489.5318 0.02 1 490.3499 0.10 7 491.3329 0.09 6 492.5543 0.38 25 493.4977 0.58 39 494.5803 0.35 23 495.5200 0.12 8 496.0266 0.04 3 496.3028 0.04 3 497.5605 0.01 1 498.0633 0.02 1 498.7668 0.04 3 499.3094 0.04 3 499.6134 0.02 1 500.2256 0.04 3 501.3864 0.03 2 501.7244 0.02 1 503.2571 0.07 5 503.8596 0.04 3 504.3825 0.04 3 504.7185 0.08 5 505.1699 0.04 3 505.7543 0.08 5 506.0819 0.08 5 506.4651 0.08 5 507.5491 1.08 72 508.5301 5.81 388 509.5448 11.13 743 510.6609 0.29 19 511.1098 0.14 9 511.4495 0.06 4 512.5897 0.04 3 513.1121 0.02 1 513.8690 0.08 5 514.5306 0.04 3 515.6174 0.04 3 516.2135 0.03 2 516.5255 0.02 1 517.7437 0.05 3 518.1968 0.02 1 518.7652 0.03 2 519.3734 0.06 4 520.5581 0.09 6 521.5163 0.24 16 522.1505 0.06 4 522.5302 0.05 3 523.2957 0.01 1 523.7092 0.02 1 525.0037 0.01 1 525.4194 0.03 2 526.0856 0.04 3 526.5808 0.01 1 527.2670 0.03 2 527.7742 0.03 2 529.3555 0.05 3 530.3005 0.07 5 531.5380 0.07 5 531.9837 0.02 1 532.5249 0.08 5 533.0403 0.03 2 533.5477 0.10 7 534.4631 0.14 9 535.6095 0.14 9 536.5509 0.14 9 536.9349 0.05 3 537.5471 0.06 4 538.3540 0.04 3 538.6104 0.04 3 539.3519 0.01 1 540.0854 0.04 3 541.1390 0.01 1 543.2486 0.01 1 543.6821 0.06 4 544.2090 0.01 1 545.5375 0.01 1 545.9750 0.04 3 546.5359 0.05 3 547.2917 0.06 4 547.9919 0.04 3 548.6384 0.08 5 548.9407 0.05 3 549.5554 0.15 10 550.5462 0.59 39 551.6106 4.16 278 552.5975 0.74 49 554.0582 0.07 5 554.7766 0.01 1 555.2383 0.01 1 556.1479 0.01 1 556.9958 0.05 3 557.5133 0.07 5 558.4091 0.07 5 558.8232 0.02 1 559.4821 0.03 2 560.5393 0.07 5 560.9056 0.04 3 561.4412 0.09 6 561.9848 0.05 3 562.6400 0.10 7 563.4843 0.01 1 564.1016 0.12 8 564.8046 0.13 9 566.6350 0.65 43 567.5649 0.34 23 568.6379 0.20 13 569.3693 0.05 3 570.4782 0.01 1 571.6052 0.05 3 572.5115 0.09 6 573.1099 0.04 3 573.4816 0.03 2 574.3384 0.05 3 575.7639 0.06 4 576.4120 0.02 1 577.4022 0.05 3 577.7740 0.04 3 578.0106 0.03 2 578.6589 0.03 2 578.9870 0.02 1 579.5180 0.01 1 580.7709 0.04 3 581.5784 0.03 2 582.0438 0.04 3 583.4640 0.04 3 583.8957 0.01 1 584.3293 0.05 3 585.0117 0.05 3 586.5595 0.09 6 587.4111 0.04 3 588.4815 0.05 3 588.9571 0.01 1 589.4586 0.07 5 589.7133 0.04 3 590.6844 0.07 5 591.3770 0.05 3 592.5015 0.19 13 593.3414 0.06 4 594.1077 0.07 5 594.7089 0.04 3 596.5901 3.15 210 597.6672 0.09 6 598.9196 0.04 3 599.5089 0.03 2 601.0263 0.05 3 601.5500 0.04 3 601.8248 0.02 1 602.4940 0.08 5 603.4022 0.01 1 603.7925 0.02 1 604.4817 0.05 3 605.2087 0.08 5 606.0035 0.02 1 606.3979 0.03 2 607.6310 0.05 3 608.9020 0.04 3 609.9978 0.03 2 610.5218 0.08 5 612.6778 0.06 4 613.0743 0.03 2 613.4869 0.02 1 614.0728 0.04 3 614.5551 0.04 3 615.4440 0.03 2 616.4517 0.06 4 616.9710 0.04 3 617.8345 0.03 2 618.4313 0.02 1 619.1576 0.04 3 619.5337 0.03 2 620.1904 0.08 5 621.4540 0.09 6 622.6739 0.09 6 623.8859 0.04 3 624.2422 0.04 3 624.6682 0.06 4 625.2911 0.04 3 626.2088 0.04 3 626.4476 0.03 2 626.7422 0.04 3 627.3514 0.02 1 627.8829 0.05 3 628.3826 0.08 5 628.9440 0.06 4 629.5114 0.05 3 630.0948 0.06 4 630.5726 0.03 2 631.6119 0.08 5 632.7350 0.09 6 633.9556 0.08 5 634.8020 0.03 2 635.2800 0.09 6 635.9492 0.08 5 636.6940 0.09 6 637.4927 0.03 2 637.8811 0.05 3 638.7435 0.18 12 639.5921 0.09 6 640.4208 0.07 5 641.5483 0.04 3 642.1619 0.01 1 642.5604 0.06 4 643.2712 0.02 1 644.1965 0.02 1 644.5826 0.06 4 644.9249 0.04 3 645.3468 0.03 2 646.4932 0.09 6 646.9091 0.06 4 647.2017 0.04 3 647.9938 0.04 3 648.5134 0.03 2 649.0846 0.14 9 649.7256 0.18 12 650.6910 0.82 55 651.6167 0.16 11 652.4827 0.05 3 653.1138 0.07 5 653.9221 0.06 4 655.1685 0.17 11 656.4349 0.12 8 656.8610 0.07 5 657.5320 0.05 3 658.3804 0.08 5 659.0953 0.09 6 659.4478 0.01 1 659.9477 0.03 2 660.2345 0.04 3 660.5193 0.02 1 660.9993 0.08 5 661.8278 0.03 2 662.1703 0.03 2 662.6703 0.09 6 663.0328 0.02 1 663.7360 0.05 3 664.7319 0.08 5 665.5766 0.05 3 666.6921 0.21 14 669.1980 0.45 30 671.0132 0.44 29 672.6497 0.41 27 675.3024 0.51 34 677.0167 0.35 23 678.7590 0.30 20 680.4000 0.43 29 681.3827 0.41 27 682.8548 0.48 32 684.4642 7.85 524 685.3615 0.24 16 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